HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glutaric anhydride → HCID 19040702, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glutaric anhydride | HCID 7940 | — |
| Reactant | 1-(4-Nitrophenyl)-4-methyl-7,8-methylenedioxy-3,4-dihydro-5H-2,3-benzodiazepine | HCID 10336422 | — |
| Product | HCID 19040702 | HCID 19040702 | — |
Reaction Steps
By using the product of Example 26 as starting material and performing the acylation according to Example 14 with glutaric acid anhydride, finally recrystallizing the raw product from ethanol the pure aimed product was obtained, m.p.: 148°-150° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05604223 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-c56becbfc1154915a572afe0d64f6b9f |
| Source note | uspto-grants-1997_02 |