HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 15228889, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | 2-Oxo-1,2-dihydroquinoline-3,4-dicarboxylic acid | HCID 804596 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 15228889 | HCID 15228889 | — |
Reaction Steps
A mixture of 2(1H)-Oxo-quinoline-3,4-dicarboxylic acid (2 g), phosphorous oxychloride (4 g) and dry chloroform (30 mL) was heated at reflux for 2 h. The solvent and excess reagents are removed in vacuo and the residue was treated with ice water to afford Furo[3,4-c]quinoline-1,3,4(5H)-trione as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05604235 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-e78bb8829bec478299a81c30649d0828 |
| Source note | uspto-grants-1997_02 |