Benzyl Bromide → HCID 178481934, compound

Participants

Reaction Steps

A reaction mixture of 2.3 g (14.83 mmol) of 5-(1,3-dioxolan-2-yl)-1-methyl-1,2,4-triazole and 2.53 g (14.83 mmol) of benzyl bromide was heated on a steam-bath with stirring for 48 h. The mixture was cooled to room temperature, triturated with ethyl acetate and decanted to afford 3.1 g (64.1%) of 4-benzyl-5-(1,3-dioxolan-2-yl)-1-methyl-1,2,4-triazolium bromide (Formula VI: A=1-methyl-1,2,4-triazolo; Y=5-(1,3-dioxolan-2-yl); R1 =R6 =H; Z- =Br-).

Provenance & Evidence