HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexane → 13-Phenyltridecanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexane | HCID 8058 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Product | 13-Phenyltridecanol | HCID 21849314 | — |
Reaction Steps
melting point=34°-36° C. Rf value: 0.24 (ethyl acetate:hexane=1:5); 1H-NMR (CDCl3 /TMS) δ: 1.28 & 1.57 (23H, 2br.s), 2.62 (2H, t, J=7.5 Hz), 3.65 (2H, t, J=6 Hz), 7.23 (5H, m); IR(KBr): 3344, 3259, 2918, 2848, 1468 cm-1 ; MS(EI): 276 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05604229 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-4dbc9b372c41443c8fb26231df3e0d8d |
| Source note | uspto-grants-1997_02 |