HCID 15289114, compound → HCID 15289115, compound

HRID 1451712Notes

Reaction equation

HRID 1451712 reaction equation
[CH3:1][N:2]([CH3:16])[C:3]12[CH2:13][CH2:12][CH:9]([CH:10]=[CH:11]1)[CH:8]1[CH:4]2[C:5](=O)[NH:6][C:7]1=O.[H-].[H-].[H-].[H-].[Li+].[Al+3]>>[CH3:1][N:2]([CH3:16])[C:3]12[CH2:13][CH2:12][CH:9]([CH:10]=[CH:11]1)[CH:8]1[CH:4]2[CH2:5][NH:6][CH2:7]1

Participants

3

Reactant 2

HCID 15289114HCID 15289114, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 15289115HCID 15289115, compound

Procedure

12 g (54.5 mmol) of 1-dimethylamino-4-azatricyclo-[5.2.2.02,6 ]undec-8-ene-3,5-dione are reduced with LiAlH4 as described under Z 1-B and the mixture is worked up accordingly.

Sources & evidence

ORD record
ord-466747143950431284ada5e30562018b
Source dataset
uspto-grants-1997_02
Patent number
US05605910

Reaction notes

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