173019-82-4 → HCID 19973050, compound

HRID 1451827Notes

Reaction equation

HRID 1451827 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[S:9][C:8]([S:10][CH:11]3[S:15][C:14](=[O:16])[NH:13][C:12]3=[O:17])=[N:7][C:6]=2[CH:18]=1.[Cl:19][C:20]1[CH:25]=[CH:24][C:23]([C:26]#[C:27][CH2:28]Br)=[CH:22][CH:21]=1.FC1C=C(C#CCBr)C=C(F)C=1>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[S:9][C:8]([S:10][C:11]3([CH2:28][C:27]#[C:26][C:23]4[CH:24]=[CH:25][C:20]([Cl:19])=[CH:21][CH:22]=4)[S:15][C:14](=[O:16])[NH:13][C:12]3=[O:17])=[N:7][C:6]=2[CH:18]=1

Participants

4

Reactant 3

HCID 10513607173019-82-4HCID 19973047HCID 19973047, compoundHCID 19973049HCID 19973049, compound

Product 1

HCID 19973050HCID 19973050, compound

Procedure

Prepared from 5-(5-chloro-benzothiazol-2-ylsulfanyl)-thiazolidine-2,4-dione, (III), Example 88 and [3-(4-chlorophenyl)-prop-2-ynyl]-bromide of formula (IX), Example 21: mp 187°-188° C.; Anal. Calc. for C19H10Cl2N2O2S3 : C, 49.04; H, 2.17; N, 6.02; Found: C, 48.94; H, 2.31; N, 6.21.

Sources & evidence

ORD record
ord-794d49ca7c2d4e3d9fff40d091726f9d
Source dataset
uspto-grants-1997_02
Patent number
US05605918

Reaction notes

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