HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodopropane → HCID 22923348, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodopropane | HCID 33643 | — |
| Reactant | 3-(1-Ethoxycarbonyl-4-piperidinyl)-1,2,3,4-tetrahydro-6-methyl-2,4-dioxoquinazoline | HCID 21851246 | — |
| Product | HCID 22923348 | HCID 22923348 | 97% |
Reaction Steps
The procedure similar to that described in Example 1 was repeated, except that 1.0 g (3.02 mmol) of 3-(1-ethoxycarbonyl-4-piperidinyl)-1,2,3,4-tetrahydro-6-methyl-2,4-dioxoquinazoline (Compound f) was used in place of Compound 24 and propyl iodide was used in place of methyl iodide, whereby 1.09 g (yield: 97%) of Compound c was obtained as a colorless oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05605900 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-5764ca4e54274a97a247012e935ef6a8 |
| Source note | uspto-grants-1997_02 |