関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Benzylamine | HCID 7504 | — |
| 反応物 | Ethyl (2-methylacryloyl)carbamate | HCID 13628540 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | N-[(benzylamino)carbonyl]-2-methylacrylamide | HCID 639951 | 42.6% |
反応手順
A reaction vessel was charged with 78.5 g of ethyl N-methacryloylcarbamate and 53.5 g of benzylamine to which 100 g of toluene were added and heated at 100° C. for 30 minutes, The resulting mixture was condensed under reduced pressure and isolated by column chromatography to obtain 46.4 g of N-benzyl-N'-methacryloyl urea having a melting point of 96°-98° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05606096 |
|---|
| 出典データセット | uspto-grants-1997_02 |
|---|
| ORD ID | ord-a8d45f9f89c844ebb793f09535acb143 |
|---|
| 出典メモ | uspto-grants-1997_02 |
|---|
