HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1452126Generated: October 25, 2026
Aniline → 2-propenamide, 2-methyl-N-((phenylamino)carbonyl)-
https://huagongshe.com/reaction/1452126
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Ethyl (2-methylacryloyl)carbamate | HCID 13628540 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2-propenamide, 2-methyl-N-((phenylamino)carbonyl)- | HCID 231918 | 45.5% |
Reaction Steps
A reaction vessel was charged with 78.5 g of ethyl N-methacryloylcarbamate and 46.5 g of aniline to which 100 g of toluene were added and heated at 120° C. for 30 minutes. The resulting mixture was condensed under reduced pressure and isolated by column chromatography to obtain 46.4 g of N-methacryloyl-N'-phenyl urea having a melting point of 165° to 166° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05606096 |
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| Source dataset | uspto-grants-1997_02 |
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| ORD ID | ord-59ffe58a053948f3ad86702b888546eb |
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| Source note | uspto-grants-1997_02 |
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