HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 15344573, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 15344572 | HCID 15344572 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 15344573 | HCID 15344573 | — |
Reaction Steps
A solution of 1.1 ml of thionyl chloride in 2 ml of chloroform was added to a boiling solution of 3.37 g of Intermediate XXXVI in 20 ml of chloroform. After stirring for 90 minutes under reflux, the solvent was removed in vacuo and the residue was crystallized from acetonitrile to give 3 g of pure title compound, m.p. (188) 193°-194° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05605896 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-d646325291bd4d3d876d47e2e9bd2595 |
| Source note | uspto-grants-1997_02 |