HCID 19972376, compound → HCID 19972489, compound

HRID 1452325Notes

Reaction equation

HRID 1452325 reaction equation
[ClH:1].[CH3:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[N:9]1[CH2:14][CH2:13][N:12]([CH2:15][C:16]([C:18]2[C:27]3[O:26][C:25]([C:28]4[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=4)=[C:24]([CH3:34])[C:23](=[O:35])[C:22]=3[CH:21]=[CH:20][CH:19]=2)=[O:17])[CH2:11][CH2:10]1>C(O)C>[ClH:1].[OH:17][CH:16]([C:18]1[C:27]2[O:26][C:25]([C:28]3[CH:29]=[CH:30][CH:31]=[CH:32][CH:33]=3)=[C:24]([CH3:34])[C:23](=[O:35])[C:22]=2[CH:21]=[CH:20][CH:19]=1)[CH2:15][N:12]1[CH2:13][CH2:14][N:9]([C:4]2[CH:5]=[CH:6][CH:7]=[CH:8][C:3]=2[CH3:2])[CH2:10][CH2:11]1

Participants

3

Reactant 1

HCID 19972376HCID 19972376, compound

Product 1

HCID 19972489HCID 19972489, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

This compound was prepared according to Example 17, but starting from the compound prepared in Example 2, rather than that prepared in Example 1. m.p. 257°-258° C. (ethanol).

Workup

  1. customThis compound was prepared
  2. customprepared in Example 1

Sources & evidence

ORD record
ord-bbf7e36690614f9ea3613e28c9b03414
Source dataset
uspto-grants-1997_02
Patent number
US05605896

Reaction notes

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