HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 10491195, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Acetylacetone | HCID 31261 | — |
| Reactant | Theophyllidine | HCID 12443409 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 10491195 | HCID 10491195 | — |
Reaction Steps
Theophyllidine (hydrochloride), 27.0 g (0.142 mol), from step 1, was heated in 1400 ml methanol under reflux for 5 hours with acetylacetone, 28.7 g (0.284 mol), and 20 g concentrated hydrochloric acid. The solvent was then removed on the rotary evaporator and the yellow residue was purified by recrystallization from ethanol/diethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07473280B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-dd5cb02dd6a64ffb95c62011bc3c3bac |
| Source note | uspto-grants-2009_01 |