HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1452524Generated: November 1, 2026
Dimethylformamide dimethyl acetal → 1-Penten-3-one, 1-(dimethylamino)-4,4-dimethoxy-
https://huagongshe.com/reaction/1452524
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 3,3-Dimethoxy-2-butanone | HCID 140871 | — |
| Product | 1-Penten-3-one, 1-(dimethylamino)-4,4-dimethoxy- | HCID 566811 | 99.5% |
Reaction Steps
A mixture of 100 g of 3,3-dimethoxy-2-butanone and 99.2 g of N,N-dimethylformamide dimethylacetal was stirred at 100° C. for 42 hours. After cooling the reaction mixture, the mixture was concentrated under reduced pressure to give 141 g of 1-dimethylamino-4,4-dimethoxy-1-penten-3-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07473695B2 |
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| Source dataset | uspto-grants-2009_01 |
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| ORD ID | ord-98a95ce767734836a021a5adb868c241 |
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| Source note | uspto-grants-2009_01 |
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