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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1452541Generated: October 31, 2026

Boron trifluoride etherate → HCID 10216587, compound

https://huagongshe.com/reaction/1452541

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBoron trifluoride etherateHCID 8000—
ReactantTriethylsilaneHCID 12052—
ReactantHCID 9909725HCID 9909725—
ProductHCID 10216587HCID 10216587—

Reaction Steps

The title compound was prepared from N-(4-{1-hydroxy-1-[1-(2-methox-yethyl)-1H-pyrrol-2-yl]-ethyl}-phenyl)-N-methyl-benzenesulfonamide (Example 1) using triethylsilane and boron trifluoride diethyl etherate as described in Example 88 of U.S. application Ser. No. 10/354,922, now U.S. Pat. No. 7,071,358, and provided below as Preparative Example B.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07473703B2
Source datasetuspto-grants-2009_01
ORD IDord-ecc19134f595408fab1babc0365176e8
Source noteuspto-grants-2009_01