HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 11108761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Pyridinium hydrochloride | HCID 21584435 | — |
| Reactant | HCID 21864274 | HCID 21864274 | — |
| Product | HCID 11108761 | HCID 11108761 | — |
Reaction Steps
81.68 g (0.300 mol) methyl(pentafluorophenyl)dimethoxysilane, 109 mL (1.50 mol, 178.4 g) thionylchloride and 3.69 g (0.0319 mol) pyridinium hydrochloride are refluxed and stirred for 16 h. Excess of SOCl2 is evaporated and methyl(pentafluorophenyl)dichlorosilane isolated by vacuum-distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07473650B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-578ea39d30f7408daf9e44c8fd09045b |
| Source note | uspto-grants-2009_01 |