Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Propionic Acid | HCID 1032 | — |
| Reactant | P-Toluenesulfonylhydrazide | HCID 15303 | — |
| Reactant | 1,1-Dichloro-2-butanone | HCID 3083774 | — |
| Product | HCID 57526999 | HCID 57526999 | — |
Reaction Steps
1,1-Dichlorobutan-2-one (CAS Registry Number 2648-56-8) (210 mg, 1.49 mmol) and 4-methylbenzenesulfonohydrazide (268 mg, 1.49 mmol) were added to propionic acid (3 ml), heated to 80° C. for 5 hours and then allowed to cool to room temperature overnight. Hexanes (20 ml) were added and the precipitate was filtered under nitrogen to yield the title compound (100 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07473699B2 |
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| Source dataset | uspto-grants-2009_01 |
|---|
| ORD ID | ord-537a483c62494933bd972472b08f3bed |
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| Source note | uspto-grants-2009_01 |
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