HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethynylaniline → N-(2-ethynylphenyl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethynylaniline | HCID 4153905 | — |
| Reactant | 2-Iodo-N-phenylacetamide | HCID 11207703 | — |
| Product | N-(2-ethynylphenyl)acetamide | HCID 10261360 | — |
Reaction Steps
The N-acetyl-2-ethynylaniline was prepared from 2-iodoacetanilide by Sonogashira coupling and using the same method as the synthesis of 2-ethynyl aniline. Afforded light brown solid 45% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07473786B1 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-3c4721ef89c04019925e54e9c0e98bab |
| Source note | uspto-grants-2009_01 |