Phenylacetylene → HCID 11031167, compound

Participants

Reaction Steps

The modified procedure was used to convert phenylacetylene and (E)-1-iodooctene to the title product. Purification by flash chromatography (light petroleum ether as eluent) afforded a clear oil (418 mg, 98% yield). The proton spectra obtained matches that of the analytically pure compound previously isolated (see Table 3, entry 5). 1H NMR (400 MHz, CDCl3) δ 7.42 (m, 2H), 7.28 (m, 3H), 6.24 (m, 1H), 5.66 (d, J=15.85, 1H), 2.15 (q, 2H), 1.42-1.29 (m, 8H), 0.89 (t, 3H).

Provenance & Evidence