HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dichlorobenzenethiol → 6-[2-(3-chloro-4-methoxyphenyl)ethyl]6-cyclopentyl-3-[(2,3-dichlorophenyl)thio]4-hydroxy-5,6-dihydro-2H-pyran-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dichlorobenzenethiol | HCID 140202 | — |
| Reactant | 3-Chloro-6-[2-(3-chloro-4-methoxy-phenyl)-ethyl]-6-cyclopentyl-dihydro-pyran-2,4-dione | HCID 68867451 | — |
| Product | 6-[2-(3-chloro-4-methoxyphenyl)ethyl]6-cyclopentyl-3-[(2,3-dichlorophenyl)thio]4-hydroxy-5,6-dihydro-2H-pyran-2-one | HCID 58762572 | — |
Reaction Steps
The title compound was prepared as described in Example C(70), where 3-chloro-6-[2-(3-chloro-4-methoxyphenyl)ethyl]-6-cyclopentyldihydro-2H-pyran-2,4(3H)-dione was used in place of 3-chloro-6-[2-(5-chloro-2,4-dimethoxyphenyl)ethyl]6-cyclopentyldihydro-2H-pyran-2,4(3H)-dione and 2,3-dichlorothiophenol was used in place of 6-hydroxy-8-mercaptopurine monohydrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07473790B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-0a6760c8948c469f9c3ddff86c8f24a1 |
| Source note | uspto-grants-2009_01 |