HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Heptanamine → Benzofuran-2-carboxylic(1-propylbutyl)amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Heptanamine | HCID 38665 | — |
| Reactant | 2-Benzofurancarbonyl chloride | HCID 38949 | — |
| Product | Benzofuran-2-carboxylic(1-propylbutyl)amide | HCID 57527950 | 73% |
Reaction Steps
Prepared in a similar manner to example 1 using benzofuran-2-carbonyl chloride and heptan-4-amine. Yield: 73%. 1H NMR (500 MHz, CDCl3): a 0.93 (t, 6H, J=7.2 Hz), 1.41 (m, 8H), 3.01 (s, 3H), 4.18 (m, 1H), 6.29 (d, 1H, J=9.94 Hz), 7.20 (d, 1H, J=8.62 Hz), 7.37 (m, 2H), 7.44 (s, 1H). MS (M+H, 260).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07476399B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-e3b996cf6ce04d2ebbff0d0ad7f5708a |
| Source note | uspto-grants-2009_01 |