3,4-Dimethylbenzoic acid → 3,4-dimethyl-N-(2-methylheptan-4-yl)benzamide

Participants

Role	Name	HCID	Charge
Reactant	3,4-Dimethylbenzoic acid	HCID 12073	—
Reactant	2-Methylheptan-4-amine	HCID 14418175	—
Product	3,4-dimethyl-N-(2-methylheptan-4-yl)benzamide	HCID 57527927	—

Reaction Steps

Prepared in a similar manner to example 4 using 3,4-dimethylbenzoic acid and 2-methylheptan-4-amine (example 2a). 1H NMR (500 MHz, CDCl3): δ 0.94 (m, 9H); 1.40 (m, 5H); 1.53 (m, 1H); 1.68 (m, 1H); 2.29 (s, 3H); 2.30 (s, 3H); 4.24 (m, 1H); 5.69 (d, 1H); 7.17 (d, 1H); 7.46 (d, 1H); 7.54 (s, 1H). MS (262, M+H).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07476399B2
Source dataset	uspto-grants-2009_01
ORD ID	ord-f8d871399e9943c883624fa6e670d9f2
Source note	uspto-grants-2009_01