p-Methylphenethylamine → 3-methyl-N-(p-tolylethyl)furan-2-carboxamide

HRID 1453503Notes

Reaction equation

HRID 1453503 reaction equation

[CH3:1][C:2]1[CH:6]=[CH:5][O:4][C:3]=1[C:7]([OH:9])=O.[C:10]1([CH3:19])[CH:15]=[CH:14][C:13]([CH2:16][CH2:17][NH2:18])=[CH:12][CH:11]=1>>[CH3:1][C:2]1[CH:6]=[CH:5][O:4][C:3]=1[C:7]([NH:18][CH2:17][CH2:16][C:13]1[CH:14]=[CH:15][C:10]([CH3:19])=[CH:11][CH:12]=1)=[O:9]

Participants

3

Reactant 2

HCID 76751p-Methylphenethylamine

HCID 781273-Methyl-2-furoic acid

Product 1

HCID 575278553-methyl-N-(p-tolylethyl)furan-2-carboxamide

Procedure

Prepared in a similar manner as described in example 4 from 3-methylfuran-2-carboxylic acid and 2-p-tolylethanamine. MS (M+H, 244).

Workup

customPrepared in a similar manner

Sources & evidence

ORD record: ord-bce46029b35b464cb40578d87dea41f2
Source dataset: uspto-grants-2009_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07476399B2

Reaction notes

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