2-Pyridineethanamine → HCID 57527980, compound

HRID 1453505Notes

Reaction equation

HRID 1453505 reaction equation
[O:1]1[CH2:6][CH2:5][O:4][C:3]2[C:7]([CH2:11][NH2:12])=[CH:8][CH:9]=[CH:10][C:2]1=2.[N:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[CH2:19][CH2:20][NH2:21]>>[O:1]1[CH2:6][CH2:5][O:4][C:3]2[C:7]([CH2:11][NH:12][C:3](=[O:4])[C:2]([NH:21][CH2:20][CH2:19][C:14]3[CH:15]=[CH:16][CH:17]=[CH:18][N:13]=3)=[O:1])=[CH:8][CH:9]=[CH:10][C:2]1=2

Participants

3

Reactant 2

HCID 759192-PyridineethanamineHCID 2795040HCID 2795040, compound

Product 1

HCID 57527980HCID 57527980, compoundYield 50%

Procedure

Prepared in a similar manner to example 122 using (2,3-dihydrobenzo[b][1,4]dioxin-5-yl)methanamine, ethyl oxalyl chloride, and 2-(2-pyridinyl)ethyl amine; yield 50%; m/e=342 [M+1].

Sources & evidence

ORD record
ord-bc919a037de04d31b608970da726622d
Source dataset
uspto-grants-2009_01
Patent number
US07476399B2

Reaction notes

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