Benzo-1,3-dioxole-5-methylamine → HCID 57331136, compound

HRID 1453506Notes

Reaction equation

HRID 1453506 reaction equation
[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH2:10][NH2:11])=[CH:9][C:4]=2[O:3][CH2:2]1.[N:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[CH2:18][CH2:19][NH2:20]>>[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH2:10][NH:11][C:4](=[O:3])[C:5]([NH:20][CH2:19][CH2:18][C:13]3[CH:14]=[CH:15][CH:16]=[CH:17][N:12]=3)=[O:1])=[CH:9][C:4]=2[O:3][CH2:2]1

Participants

3

Reactant 2

HCID 75799Benzo-1,3-dioxole-5-methylamineHCID 759192-Pyridineethanamine

Product 1

HCID 57331136HCID 57331136, compoundYield 35%

Procedure

Prepared in a similar manner to example 125 using benzo[d][1,3]dioxol-5-ylmethanamine, ethyl oxalyl chloride, and 2-(2-pyridinyl)ethyl amine; yield 35%; m/e=328 [M+1].

Sources & evidence

ORD record
ord-7d88eda949184ca1845e69c38cb4d504
Source dataset
uspto-grants-2009_01
Patent number
US07476399B2

Reaction notes

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