HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzimidazole → HCID 178478376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzimidazole | HCID 5798 | — |
| Reactant | 2,6-Dichloropurine | HCID 5324412 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 178478376 | HCID 178478376 | 26.2% |
Reaction Steps
8 g of 2,6-dichloropurine, 150 ml of butanol and 5.5 g of benzimidazole are mixed and brought to a temperature of 80° C. for approximately 17 hours. The mixture is allowed to return to ambient temperature. Partial drying, washing with ethyl ether and drying under vacuum are carried out, and 3 g of expected product are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07476670B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-f1fd243e3f1d435bafe68fa79e3c582e |
| Source note | uspto-grants-2009_01 |