HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1453608Generated: October 29, 2026
HCID 178511674, compound → HCID 178511668, compound
https://huagongshe.com/reaction/1453608
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 178511674 | HCID 178511674 | — |
| Reactant | HCID 178526437 | HCID 178526437 | — |
| Product | HCID 178511668 | HCID 178511668 | — |
Reaction Steps
56 g of product obtained in stage 1 above are mixed with 140 g of trans-1,4-diaminocyclohexane, and the mixture is then heated at 140° C. for approximately 55 hours. The mixture is allowed to return to ambient temperature. Purification is carried out by chromatography on silica with a CH2Cl2-MeOH—NH4OH: 85-15-1.5 mixture for eluent. 19.7 g of product are recovered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07476670B2 |
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| Source dataset | uspto-grants-2009_01 |
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| ORD ID | ord-3933cc4624d544448e14e02547a11caa |
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| Source note | uspto-grants-2009_01 |
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