3-Chloro-1-propanol → HCID 69052270, compound

HRID 1453666Notes

Reaction equation

HRID 1453666 reaction equation
[N:1]([C:4]1[CH:9]=[CH:8][C:7]([N+:10]([O-:12])=[O:11])=[CH:6][C:5]=1[CH3:13])=[C:2]=[O:3].[Cl:14][CH2:15][CH2:16][CH2:17][OH:18]>C1(C)C=CC=CC=1>[CH3:13][C:5]1[CH:6]=[C:7]([N+:10]([O-:12])=[O:11])[CH:8]=[CH:9][C:4]=1[NH:1][C:2](=[O:3])[O:18][CH2:17][CH2:16][CH2:15][Cl:14]

Participants

4

Reactant 2

HCID 123133-Chloro-1-propanolHCID 42964562-Methyl-4-nitrophenyl isocyanate

Product 1

HCID 69052270HCID 69052270, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

Prepared analogously to Example 51b from 4-isocyanato-3-methyl-1-nitro-benzene and 3-chloro-propan-1-ol in toluene.

Sources & evidence

ORD record
ord-84b36b0772a849fcb8c498407fec8bdc
Source dataset
uspto-grants-2009_01
Patent number
US07476663B2

Reaction notes

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