Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → Ethyl (4-iodophenyl)acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 4-Iodophenylacetic acid | HCID 137214 | — |
| 생성물 | Ethyl (4-iodophenyl)acetate | HCID 14974990 | 90% |
반응 단계
4-Iodophenylacetic acid (3 g), ethanol (20 mL) and conc. H2SO4 (5 mL) were refluxed overnight. Ca. 15 mL ethanol was then evaporated, the residue was extracted with dichloromethane (3×100 mL), the combined organic extracts were washed with sat. aq. NaHCO3, dried over Na2SO4 and evaporated in vacuo to afford 2.97 g (90%) of 121JP58 as a yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07476682B2 |
| 출처 데이터셋 | uspto-grants-2009_01 |
| ORD ID | ord-b0f996641a5a41ca86920a78dddbc367 |
| 출처 메모 | uspto-grants-2009_01 |