HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nicotinic acid, hydrazide → 3-(4-Methyl-5-(methylsulfonyl)-4H-1,2,4-triazol-3-yl)pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nicotinic acid, hydrazide | HCID 11112 | — |
| Reactant | 4-(4-Methyl-5-(methylsulfonyl)-4H-1,2,4-triazol-3-yl)pyridine | HCID 22151477 | — |
| Product | 3-(4-Methyl-5-(methylsulfonyl)-4H-1,2,4-triazol-3-yl)pyridine | HCID 46928334 | — |
Reaction Steps
The title compound was prepared analogously to 4-[4-methyl-5-(methylsulfonyl)-4H-1,2,4-triazol-3-yl]pyridine as described herein, via the corresponding sequence consisting of the corresponding steps, by starting from nicotinohydrazide instead of isonicotinohydrazide. 1H NMR: 3.59 (s, 3H), 3.99 (s, 3H), 7.52 (m, 1H), 8.02 (dt, 1H), 8.83 (dd, 1H), 8.91 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07476684B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-34d846db096d4ff39a7df60442d4a5dc |
| Source note | uspto-grants-2009_01 |