HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86602198, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Benzenesulfonyl chloride, 2,4-dichloro- | HCID 204419 | — |
| Reactant | 2-Amino-m-cresol | HCID 3014138 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86602198 | HCID 86602198 | — |
Reaction Steps
To a mixture of 2,4-dichlorobenzenesulfonyl chloride (20.2 g, 82.3 mmol) and 2-amino-m-cresol (11 g, 89.4 mmol) in 200 mL of methylene chloride, triethylamine (8.5 g, 83.4 mmol) was added dropwise at 5° C. The mixture was stirred at ambient temperature for 16 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07476690B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-7fb5297cf8fb41a684d6fdaaeed0d2b5 |
| Source note | uspto-grants-2009_01 |