HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-bromobenzoate → 3-(5-Bromo-2-pyridyl)-3-pentanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-bromobenzoate | HCID 12070 | — |
| Reactant | 4-Bromo-2-methylphenyl acetate | HCID 60026774 | — |
| Reactant | Ethyl-5-bromo-2-carboxypyridine | HCID 67144082 | — |
| Reactant | HCID 178418443 | HCID 178418443 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 3-(5-Bromo-2-pyridyl)-3-pentanol | HCID 11687386 | — |
Reaction Steps
The title compounds were prepared using methyl-3-bromobenzoate, methyl-4-bromophenyl acetate, ethyl-5-bromo-2-carboxypyridine or ethyl-5-bromo-2-carboxypyridine and ethyl magnesium bromide with methylene chloride as solvent, respectively, but otherwise followed the procedure detailed for Preparation 36.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07479559B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-af4c73c20ef94e7181eed01fd20518e4 |
| Source note | uspto-grants-2009_01 |