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HRID1454521

反应详情

EQUATION

反应方程式

HRID 1454521 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)NS(=O)(=O)c1cccc(B2OC(C)(C)C(C)(C)O2)c1
HCID58169119

未命名化合物

结构：COc1c(Br)cc(S(=O)(=O)NC(C)=O)cc1C=O
HCID86607697

未命名化合物

PRODUCTS

生成物

1
结构：COc1c(C=O)cc(S(=O)(=O)NC(C)=O)cc1-c1cccc(S(=O)(=O)NC(C)(C)C)c1
HCID86607706

未命名化合物

收率 51.6%

PROCEDURE

实验过程

Proceeding as in Reference 19, but substituting N-acetyl-3-bromo-5-formyl-4-methoxy-benzenesulfonamide (335 mg, 1.0 mmol) and N-tert-butyl-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)benzenesulfonamide (373 mg, 1.1 mmol), gave N-acetyl-N′-tert-butyl-5-formyl-6-methoxy-biphenyl-3,3′-disulfonamide (242 mg) as a pale yellow oil.