HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Difluorobenzenesulfonyl chloride → 2,5-Difluoro-N-[6-(4-fluoro-benzyloxymethyl)-pyridin-2-yl]-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Difluorobenzenesulfonyl chloride | HCID 2736911 | — |
| Reactant | 6-(4-Fluoro-benzyloxymethyl)-pyridin-2-ylamine | HCID 68845140 | — |
| Product | 2,5-Difluoro-N-[6-(4-fluoro-benzyloxymethyl)-pyridin-2-yl]-benzenesulfonamide | HCID 11560547 | — |
Reaction Steps
This material was prepared in analogy to example 1 from 6-(4-fluoro-benzyloxymethyl)-pyridin-2-ylamine (0.058 g) and 2,5-difluoro-benzenesulfonyl chloride (0.058 g) as a light yellow gum (0.075 g). MS (ESI−): 407.2 ([M−H]−)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482341B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-131c2a2827894822b8fd64db6cdd83d9 |
| Source note | uspto-grants-2009_01 |