HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-2-methylbenzenesulfonyl chloride → 3-Chloro-N-(5-methoxymethyl-6-methyl-pyridin-2-yl)-2-methyl-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-2-methylbenzenesulfonyl chloride | HCID 522734 | — |
| Reactant | 5-(Methoxymethyl)-6-methylpyridin-2-amine | HCID 68845551 | — |
| Product | 3-Chloro-N-(5-methoxymethyl-6-methyl-pyridin-2-yl)-2-methyl-benzenesulfonamide | HCID 68840752 | — |
Reaction Steps
This material was prepared in analogy to example 1 from 5-methoxymethyl-6-methyl-pyridin-2-ylamine (0.058 g) and 3-chloro-2-methyl-benzenesulfonyl chloride (0.094 g) as an off-white foam (0.093 g). MS (ESI−): 339.0 ([M−H]−)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482341B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-a0a8d60a3f6c4a0f8e44caa886326015 |
| Source note | uspto-grants-2009_01 |