HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloro-5-methylbenzene-1-sulphonyl chloride → 2,4-Dichloro-5-methyl-N-[6-(2,2,2-trifluoro-ethoxymethyl)-pyridin-2-yl]-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloro-5-methylbenzene-1-sulphonyl chloride | HCID 119914 | — |
| Reactant | 6-(2,2,2-Trifluoro-ethoxymethyl)-pyridin-2-ylamine | HCID 68845375 | — |
| Product | 2,4-Dichloro-5-methyl-N-[6-(2,2,2-trifluoro-ethoxymethyl)-pyridin-2-yl]-benzenesulfonamide | HCID 68846384 | — |
Reaction Steps
This material was prepared in analogy to example 1 from 6-(2,2,2-Trifluoro-ethoxymethyl)-pyridin-2-ylamine (0.08 g) and 2,4-dichloro-5-methyl-benzenesulfonyl chloride (0.11 g) as a light yellow gum (0.095 g). MS (ESI−): 427.1 ([M−H]−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482341B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-5c18f8527f314738bafa3eba296252a7 |
| Source note | uspto-grants-2009_01 |