HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Bromomethyl)-3-chlorobenzene → N-[6-(3-Chloro-benzyloxymethyl)-pyridin-2-yl]-2,2-dimethyl-propionamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Bromomethyl)-3-chlorobenzene | HCID 69838 | — |
| Reactant | N-[6-(Hydroxymethyl)pyridin-2-yl]-2,2-dimethylpropanamide | HCID 21782926 | — |
| Product | N-[6-(3-Chloro-benzyloxymethyl)-pyridin-2-yl]-2,2-dimethyl-propionamide | HCID 68842609 | — |
Reaction Steps
This material was prepared in analogy to example 86 step A] from N-(6-hydroxymethyl-pyridin-2-yl)-2,2-dimethyl-propionamide (0.73 g) and 3-chlorobenzyl bromide as a yellow oil (0.75 g). MS (ESI): 332.2 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482341B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-ab0bfdc546334b35a27bf4dd271c68de |
| Source note | uspto-grants-2009_01 |