Allyl Alcohol → HCID 86602453, compound

Participants

Reaction Steps

To the subtitle product of step ii) (1.0 g) in toluene was added allyl alcohol (0.23 g), sodium hydroxide (0.16 g) and benzyltriethylammonium chloride (10 mg). The mixture was stirred at room temperature for 2 h before sodium hydroxide solution (10 ml, 1M) was added the organics extracted with EtOAc (2×50 ml). The combined organics were washed with brine (20 ml) and dried (MgSO4). The solid was filtered and the filtrate evaporated to dryness to yield the subtitle compound as a white solid. Yield 1.0 g

Provenance & Evidence