Hydrazinecarboxaldehyde → HCID 68954223, compound

HRID 1455283Notes

Reaction equation

HRID 1455283 reaction equation
[C:1]([NH:4][NH:5][C:6](=[O:26])[CH2:7][N:8]1[C:12]([CH2:13][CH3:14])=[C:11]([O:15][C:16]2[CH:21]=[CH:20][C:19]([C:22]#[N:23])=[CH:18][CH:17]=2)[C:10]([CH2:24][CH3:25])=[N:9]1)(=[O:3])C.C(C1C=CC(OC2C(CC)=NN(CC(O)=O)C=2CC)=CC=1)#N.C(NN)=O>>[C:22]([C:19]1[CH:18]=[CH:17][C:16]([O:15][C:11]2[C:10]([CH2:24][CH3:25])=[N:9][N:8]([CH2:7][C:6]([NH:5][NH:4][CH:1]=[O:3])=[O:26])[C:12]=2[CH2:13][CH3:14])=[CH:21][CH:20]=1)#[N:23]

Participants

4

Reactant 3

HCID 12229HydrazinecarboxaldehydeHCID 68919233HCID 68919233, compoundHCID 68955800HCID 68955800, compound

Product 1

HCID 68954223HCID 68954223, compoundYield 51%

Procedure

The title compound (290 mg, 51%) was prepared by a similar method to that describe for the acetohydrazide of step (b) of Example 140 using the acid of step (a) of Example 140 and formic hydrazide as the starting materials.

Sources & evidence

ORD record
ord-3c3b1f7eab8c4ba29926da2b538866be
Source dataset
uspto-grants-2009_01
Patent number
US07482375B2

Reaction notes

Loading…