HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18333207, compound → HCID 18333199, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18333207 | HCID 18333207 | — |
| Solvent | Acetic acid sulfuric acid water | HCID 86597087 | — |
| Product | HCID 18333199 | HCID 18333199 | — |
Reaction Steps
Ethyl 1-ethyl-1,4-dihydro-7-fluoro-8-methoxy-4-oxo-3-quinolinecarboxylate (1.37 g, 4.7 mmol) is suspended in a mixture of acetic acid:water:sulfuric acid (8:6:1). The mixture is refluxed for 3 hours, and then cooled to room temperature. The crystals are filtered and rinsed with cold water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482454B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-cef1ff025e864f818f32379e0e1f52af |
| Source note | uspto-grants-2009_01 |