HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dibromopyridine → 3-Bromo-5-[3-(methylthio)phenyl]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dibromopyridine | HCID 69369 | — |
| Reactant | 3-(Methylthio)benzeneboronic acid | HCID 2734383 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 3-Bromo-5-[3-(methylthio)phenyl]pyridine | HCID 68954635 | — |
Reaction Steps
Prepared according to the procedure Coupling-2 using [3-(methylthio)phenyl]boronic acid and 3,5-dibromopyridine as starting material. Flash chromatography (Hex:EtOAc; 95:5-85:15) afforded the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482456B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-e7ab0e56de72400f83edbab8e009073b |
| Source note | uspto-grants-2009_01 |