HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68957422, compound → HCID 178434729, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68957422 | HCID 68957422 | — |
| Solvent | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Product | HCID 178434729 | HCID 178434729 | — |
Reaction Steps
A solution of 2-(benzyloxy)-3-(3-methyl-1,2,4-oxadiazol-5-yl)pyridine in CH2Cl2-TFA (0.25M) was stirred 15 min at 20° C. and then concentrated. The residue was diluted with EtOAc and aqueous NaHCO3. The organic extracts were washed with brine, dried over MgSO4, filtered and concentrated to afforded the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482456B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-4360481787284abebdc41a15a317f0ac |
| Source note | uspto-grants-2009_01 |