HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thionyl Chloride → 3-(3-Bromo-4-methoxyphenyl)propanoyl chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 3-(3-Bromo-4-methoxyphenyl)propanoic acid | HCID 4547608 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | 3-(3-Bromo-4-methoxyphenyl)propanoyl chloride | HCID 86605161 | — |
Reaktionsschritte
A solution of 102.4 g (0.86 mol) of thionyl chloride is added to a solution of 51.8 g (0.2 mol) of 3-(3-bromo-4-methoxyphenyl)propanoic acid in 700 ml of chloroform. The mixture is heated at reflux for 4 hours, and the solvent is then evaporated off. 53 g are obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07482484B2 |
| Quelldatensatz | uspto-grants-2009_01 |
| ORD ID | ord-0ee2744e847249628c9e61bc778d8953 |
| Quellennotiz | uspto-grants-2009_01 |