HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lawesson's reagent → HCID 22105793, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | HCID 1225859 | HCID 1225859 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 22105793 | HCID 22105793 | — |
Reaction Steps
2.5 g of product obtained in Example 21 and 5.31 g of Lawesson's reagent are dissolved in 50 ml of toluene, and the solutions maintained at reflux for 4 h. It is filtered and the solvent is evaporated off. The product is purified by chromatography on silica gel, eluting with dichloromethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05843947 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-84cabd8c2f2f4b24ad471005c85cc8d9 |
| Source note | uspto-grants-1998_12 |