Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | HCID 1225859 | HCID 1225859 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 86751977 | HCID 86751977 | — |
Reaction Steps
A solution of 10 ml of glacial acetic acid and 0.7 ml of aqueous hydrogen peroxide solution (35%) are added, with stirring, to 1 g of compound obtained in Example 21. The reaction medium is heated at 70° C. for 7 h and then concentrated under reduced pressure and at low temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05843947 |
|---|
| Source dataset | uspto-grants-1998_12 |
|---|
| ORD ID | ord-bacb57b24d3d4bc498c150229c860779 |
|---|
| Source note | uspto-grants-1998_12 |
|---|
