HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 2-(Benzyloxy)-4-bromobenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Bromo-2-hydroxybenzaldehyde | HCID 4066019 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 2-(Benzyloxy)-4-bromobenzaldehyde | HCID 15673062 | — |
Reaction Steps
Benzyl bromide (1.35 ml) was added to a mixture of 4-bromo-2-hydroxybenzaldehyde (2.07 g) and potassium carbonate (1.38 g) in DMF (20 ml) and the mixture was stirred at ambient temperature for 10 hours. The reaction mixture was poured into water (50 ml) to give 2-benzyloxy-4-bromobenzaldehyde as a solid which was filtered and dried, yield 2.88 g. The material was used in subsequent reactions without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05843942 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-5240495585e14aebba79cf7818d27b88 |
| Source note | uspto-grants-1998_12 |