HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-nitrobutyrate → HCID 717394, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-nitrobutyrate | HCID 25604 | — |
| Reactant | 3-Bromobenzaldehyde | HCID 76583 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 717394 | HCID 717394 | — |
Reaction Steps
A mixture of 3-bromobenzaldehyde (82.20 g), methyl-4-nitrobutyrate (65.3 g) and ammonium acetate (68.5 g) in ethanol (400 ml), was heated to reflux for 18 hours. The solvent was removed in vacuo and the resultant mixture triturated with ethanol (400 ml) to give the title compound as a white solid. (97.46 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05843966 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-32dcfb1ce967430398a392f0ff7d42f3 |
| Source note | uspto-grants-1998_12 |