Ethyl trifluoroacetate → HCID 22106672, compound

HRID 1456332Notes

Reaction equation

HRID 1456332 reaction equation
[CH3:1][O:2][CH2:3][CH2:4][C:5]1[S:9][CH:8]=[N:7][C:6]=1[CH3:10].[F:11][C:12]([F:19])([F:18])[C:13](OCC)=[O:14]>>[CH3:1][O:2][CH2:3][CH2:4][C:5]1[S:9][C:8]([C:13](=[O:14])[C:12]([F:19])([F:18])[F:11])=[N:7][C:6]=1[CH3:10]

Participants

3

Reactant 2

HCID 9794Ethyl trifluoroacetateHCID 11159460HCID 11159460, compound

Product 1

HCID 22106672HCID 22106672, compound

Procedure

From 5-(2-methoxyethyl)-4-methylthiazole and ethyl trifluoroacetate, following the procedure of Preparation 1. 13C Nmr (CDCl3) 15.2, 27.8, 58.6, 71.3, 116.2 (q, J 288 Hz), 142.2, 154.1, 155.8 and 173.0 (q, J 36 Hz) ppm.

Workup

  1. customthe procedure of Preparation 1

Sources & evidence

ORD record
ord-a40b2857f0624c21913bd5480a700170
Source dataset
uspto-grants-1998_12
Patent number
US05843971

Reaction notes

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