Procysteine → HCID 178460327, compound

HRID 1456345Notes

Reaction equation

HRID 1456345 reaction equation
[O:1]=[C:2]1[NH:6][C@H:5]([C:7]([OH:9])=O)[CH2:4][S:3]1.Cl.[CH3:11][CH:12]([C@H:18]1[CH2:23][CH2:22][C@H:21]([CH2:24][NH2:25])[CH2:20][CH2:19]1)[CH2:13][O:14][N+:15]([O-:17])=[O:16]>>[CH3:11][CH:12]([C@H:18]1[CH2:23][CH2:22][C@H:21]([CH2:24][NH:25][C:7]([C@@H:5]2[CH2:4][S:3][C:2](=[O:1])[NH:6]2)=[O:9])[CH2:20][CH2:19]1)[CH2:13][O:14][N+:15]([O-:17])=[O:16]

Participants

3

Reactant 2

HCID 72390ProcysteineHCID 178460326HCID 178460326, compound

Product 1

HCID 178460327HCID 178460327, compound

Procedure

91 mg of the desired-compound were obtained as a colorless oil using similar procedures to those in Example 3 by using 76.9 mg of (4R)-2-oxo-4-thiazolidinecarboxylic acid and 110 mg of trans-4-(1-methyl-2-nitroxyethyl)cyclohexylmethylamine hydrochloride.

Sources & evidence

ORD record
ord-6febb6cb33dd445697d54e00ca2757be
Source dataset
uspto-grants-1998_12
Patent number
US05843973

Reaction notes

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