HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86753399, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-methyl-1-phenylbutan-1-amine | HCID 4961833 | — |
| Reactant | HCID 23701115 | HCID 23701115 | — |
| Product | HCID 86753399 | HCID 86753399 | 96% |
Reaction Steps
The reactions and treatments of Example 5 were repeated using potassium (2R,3R)-3-ethoxycarbonyloxirane-2-carboxylate (3.97 g, 20.0 mmol.), thionyl chloride (2.86 g, 24.0 mmol), 3-methyl-1-phenylbutylamine (4.25 g, 26.0 mmol), and triethylamine (2.63 g, 26.0 mmol.), to give the desired compound as a colorless viscous oil (5.86 g, yield: 96%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05843992 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-0dd6fcfdd0dc4185b053919b66d09613 |
| Source note | uspto-grants-1998_12 |