HRID1456882

反应详情

EQUATION

反应方程式

HRID 1456882 的结构方程式

PROCEDURE

实验过程

To 4 mL trifluoroacetic acid, cooled to 0° C. and stirred under argon, was added 16 (120 mg, 0.23 mmol). After 2 h, trifluoroacetic acid was removed under reduced pressure to give 15 as an off-white solid: NMR (acetone-d6) d 4.3 (2,2H), δ7.3-8.7 (m, 12H).

WORKUP

后处理

  1. customtrifluoroacetic acid was removed under reduced pressure